Blood and urine with water or the supernatiant of viscera sample being deproteined with 6 % hclo4 solution was add 0 . 2ml gdx301 porous polymer bead and shaken to absorb the drugs in specimen . then the bead was packed into a glass column . the column was washed with 10ml water and elution was effected with dichloromethane 血、尿用水稀释,脏器用6高氯酸沉淀蛋白后,加0卫dgdx301树脂振摇,滤集树脂于小层析柱中,用水10inl淋洗,二氯甲烷洗脱,收集洗脱液sml ,挥干后用0
2.
Blood and urine with water or the supernatiant of viscera sample being deproteined with 6 % hclo4 solution was add 0 . 4ml gdx301 porous polymer bead and shaken to absorb the drugs in specimen . then the bead was packed into a glass column . the column was washed with 10ml water and elution was effected with dichloromethane 血、尿用水稀释,脏器用6高氯酸沉淀蛋白后,加0 . 4mlgdx _ ( 301 )树脂振摇,滤集树脂于小层析柱中,用水10ml淋洗,二氯甲烷洗脱,收集洗脱液sml ,挥干后用0